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Beilstein J. Org. Chem. 2011, 7, 421–425, doi:10.3762/bjoc.7.54
Graphical Abstract
Scheme 1: PLE (pig liver esterase)-catalyzed saponification of β-ketoesters 1.
Figure 1: (9E)- and (9Z)-trisporic acid B.
Scheme 2: Synthesis and PLE-catalyzed saponification of β-ketoester 1c.
Scheme 3: Synthesis of key building block (+)-7.